Laboratory simulations of the transformation of emmer wheat as a result of heating

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DOI http://dx.doi.org/10.1023/B:JTAN.0000041672.45140.e9
Reference F. Braadbaart, J. van der Horst, J.J. Boon and P.F. van Bergen, Laboratory simulations of the transformation of emmer wheat as a result of heating, J. Therm. Anal. Calorim. 77, 957-973 (2004)

Whole grains of emmer wheat were heated in a pre-heated tube oven at temperatures ranging from 130-700°C under controlled anoxic conditions for maximum 280 min. For each temperature a separate experiment was carried out. Physical properties including mass loss, thermal lag, external and internal morphology and the vitrinite reflectance, C and N content, and DTMS under CI (NH3) and EI conditions were used to monitor changes as a function of the temperature. The results show remaining starch and protein rich material up to 250°C. From 310-400°C a secondary, thermally stable, product is formed and at higher temperatures a strongly carbon enriched tertiary product.